Laboratories
|
SYNTHON has 400m2
of well-equipped
laboratories for research and development purposes and small-scale
production as well. These laboratories are designed to be used for many
physical and chemical operations, in order to develop new procedures, to
optimise existing processes and to scale up multi step procedures. |
Kilo-Lab
|
SYNTHON
has 2 kilo labs
with multi-purpose equipment for process development and for
production of fine chemicals and specialities for electronic, diagnostic
and pharmaceutical applications. |
Reactors:
|
Material |
Number
|
Volume
|
Equipped with |
|
Glass lined (1) |
2 |
100l |
Stirrer,
supply tank, reflux condenser, distillation,
water separator |
|
Glass |
2 |
60l |
stirrer,
dropping funnel, reflux condenser |
|
Glass |
1 |
25l |
stirrer,
dropping funnel, reflux condenser |
|
Glass |
3 |
25l |
stirrer,
dropping funnel, reflux condenser |
|
Double jacket glass |
1 |
30l |
multi purpose
reactor with stirrer, dropping funnel,
reflux condenser, distillation column, water separator |
|
Double jacket glass |
1 |
25l |
stirrer,
dropping funnel, reflux condenser,
reflux separator for distillation |
|
Double jacket glass |
1 |
50
l (spherical) |
stirrer,
dropping funnel, reflux condenser |
(1) Initial startup 3rd
quarter 2007. |
Autoclaves:
|
Material |
Number
|
Volume
|
Temperature /
Pressure |
|
Hastelloy (2) |
1 |
60l |
250°C/100 bar |
|
Hastelloy |
1 |
3,75l |
300 °C/200 bar |
|
Stainless steel, teflon coated |
1 |
3,75l |
300 °C/200 bar |
|
Glass |
1 |
3,00l |
-20°C - 100°C/
14 bar |
(2) Initial startup 3rd
quarter 2007. |
|
6 Thermostats: -50
°C to 200 °C (Lauda and Haake)
Rotary evaporators: 2 x 20 l (Heidolph) 1x 10 l (Bόchi)
Distillation/Rectification equipment:
6 l automatic vacuum distillation apparatus (Fischer), Sulzer packing,
100 theoretical plates
Columns for chromatography: Up to 20 cm diameter, 100 cm long
Absorbers, Filters, Dryers, Mills
Filling and bottling department for dangerous goods:
2 Denios hoods for filling of bottles up to 2.5 l
1 Denios hood (practicable) for filling and repacking of drums
Warehouses for dangerous and nondangerous goods: 200 m2
|
Outsourcing /
Cooperation partners:
|
Orgentis GmbH (reactors
from 50 to 250 l)
Organica Feinchemie GmbH (reactors from 100 to 4000 l) |
Analytical Test
Methods (from subcontractors):
HPLC
GC, GC-MS
NMR (1H-, 13C-, 19F-, 31P-)
AAS / ICP
FT-IR, Fourier-Transform
DSC |
UV/VIS
spectroscopy
Fluorescence spectrometry
Loss on drying
Titration (automatically)
Water-titration (Karl-Fischer)
Density measurements |
|
|